By J.W. Edington
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In general these test specimens must be very thin 30-40 A with a low defect density. To achieve such a thin film it is essential to vacuum evaporate the material. The sequence of events involves evaporation of an intermediate layer of silver, ~ 1000 A thick, onto a freshly cleaved {100} rocksalt substrate held at 450 oc (Bruck, 1936; Shirai, 1943; Basset, 1965). This is followed by evaporation of a thin layer 30-40 A of gold onto the silver at the same temperature. The combined silver-gold film may be floated off in distilled water, transferred to 50% nitric acid to dissolve the silver, washed in distilled water and mounted on a 200 mesh grid.