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This quantity provide you with an simply understood reference ebook on smooth analytical options. With over 950 illustrations and ninety five tables, the emphasis is at the useful instead of theoretical, describing the most typical purposes and boundaries of every strategy.
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Additional info for ASM Handbook: Volume 10: Materials Characterization (Asm Handbook)
Sample text
Blenders include rifflers in which the sample emerges from a container in preset fractions. Cone and V-blenders have been designed for mixing materials. Cones are often double and joined at their bases. Rotation produces swirling or tumbling. V-blenders achieve the same result by alternately pouring their contents from one arm to the other as the device is rotated. For best results, mixers should not be overloaded and should be operated slowly enough to produce alternate interchanges of the contents.
Sampling devices may have critical dimensions or operational parameters, such as those used for sampling respirable matter, or filters used to separate "dissolved" or particulate fractions, or in isokinetic sampling. Failure to conform to critical dimensions or operational parameters can produce erroneous results. Sampling equipment such as pumps and sieves may require calibration to verify their performance characteristics at the time of use. Sampling devices ideally should not be made of or contain the analyte of interest.
Moisture loss or gain from the time of sampling to analysis also can introduce problems. When different laboratories treat the question of moisture differently (and sometimes in an unspecified manner), disparity in results can occur. The moisture content may not be theoretically defined, but based on arbitrary considerations. Arbitrary drying procedures must be described or documented. Above all, the basis for the analytical result, such as "as-received," or dried by a specific procedure, must be stated whenever the moisture content of a sample is a significant consideration (Ref 17).